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Small-angle X-ray diffraction pattern of 40 monolayers of C17-COM-BEDT-TTF deposited from 10-4 M FeCl3 solution at pH 3.8.

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Method of structure determination includes (1) calculation of unit-cell parameters from diffraction data; (2) search for possible variants of close packing of molecules in the unit-cell; (3) minimization of interaction energy for selected variants; (4) structure choice on the basis of comparison of experimental and calculated intensities of reflections.

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